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The invention provides an improved method and apparatus for making viscous
mixtures accessible to Separation by solvent extraction by means
of dispersion. The present invention further provides a method for
preparing a dispersion. This object and others which will become
apparent as the specification progresses, are accomplished by the
invention, according to which, briefly stated, a mixture to be treated
is charged with a solvent and then sprayed to form a dispersion,
which is e.g. thereafter subject to Separation. The method comprises
charging a viscous mixture with a liquid or gaseous solvent and
spraying the homogenous solution to form a dispersion, contacting
said dispersion with a solvent for at least one component of the
mixture, dissolving at least one component of the mixture in solvent,
and separating the solvent containing at least one component from
the remaining components of the mixture. Further Steps are removing
the solvent containing at least one component from the extraction
column, separating solvent from the solvent containing at least
one component by pressure reduction and/or change in temperature,
and returning the solvent to the extraction column. The apparatus
comprises an extraction column preceded by a charging column, wherein
the upper portion of the charging column has a mixture inlet, a
solvent inlet, and a liquid distributor, and filler bodies or other
suitable inserts which increase the surface area of the mixture
to be charged.
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